KO04: Organical chemical separation (3 ECTS)

STADS: 46976177

Level


Teaching period

Spring semester

Teacher responsible
Email: ebp@ifk.sdu.dk

Timetable
There is no timetable available for the chosen semester.

Prerequisites:
None

Academic preconditions:
Chemistry A (KE04), Analytical Spectroscopy (KM01). Organic chemistry A (KO 02) must be attended simultaneously at the latest. It is recommended to take the course before Molecular Synthesis (KO 03).

Course introduction
The students should obtain practical skills in separating substance mixtures by using modern separation and purification techniques and obtain practical skills in identifying and determining the functional groups of organic substances. Through identification of IR, MS og 1H and 13C NMR spectra the students should be trained in practical analytical molecular spectroscopy including the interpretation problems implied in the fact that substances could be impure or poorly separated.

Expected learning outcome


Subject overview
Separation of substance mixtures by extraction and preparative thin layer chromatography. Determination of functional groups and equivalent weight. HPLC og GLC analysis. Identification by MS, 1H and 13C NMR og IR spectra.

Literature

• R.M. Silverstein, G.C. Bassler & T.C. Morrill: Spectrometric Identification af Organic Compounds, 5th ed., John Wiley, 1991.
  eller
• D.L. Pavia, G.M. Lampman og G.S. Kriz: Introduction to Spectroscopy, Sanders Golden Sunburst Series, 1996 (samme lærebog som i KM01).

Website
This course uses e-learn (blackboard).

Prerequisites for participating in the exam
None

Assessment and marking:
Approval of report. Passed/not passed.

Expected working hours
The teaching method is based on three phase model.

Laboratory exercises. 30 hours within the laboratorys opening hours.
Educational activities

Language
This course is taught in Danish.

Course enrollment
See deadline of enrolment.

Tuition fees for single courses
See fees for single courses.