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Dansk English

KE504: Analytical Spectroscopy (5 ECTS)

STADS: 10002101

Level
Bachelor course

Teaching period
The course begins in the autumn semester and continues in the spring semester.
1st and 3rd quarter.

Teacher responsible
Email: mip@ifk.sdu.dk

Timetable
Group Type Day Time Classroom Weeks Comment
Common I Monday 09-10 U55 35-38
Common I Monday 17-18 U55 40
Common I Tuesday 14-15 U55 35-38
Common I Wednesday 09-10 U1 35
Common I Wednesday 09-10 U55 39
Common I Thursday 08-09 U55 35
Common I Thursday 09-10 U55 36-38
Common I Friday 09-10 U55 37
S1 TE Monday 10-11 Spektroskopilokalet 36-41
S1 TL Monday 11-14 Spektroskopilokalet 36-40
S1 TE Wednesday 12-13 Spektroskopilokalet 35-39
S1 TL Thursday 12-14 Spektroskopilokalet 36-40
S3 TL Monday 14-16 Spektroskopilokalet 40
S3 TE Tuesday 08-09 Spektroskopilokalet 36-41
S3 TL Tuesday 09-12 Spektroskopilokalet 36-40
S3 TE Friday 10-11 Spektroskopilokalet 35-39
S3 TL Friday 11-13 Spektroskopilokalet 36-39
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Revison of timetable:
: F torsdag uge 39 flyttet til mandag uge 40.
: Hold S2 nedlagt.

Prerequisites:
None

Academic preconditions:
None.

Course introduction
The aim of the course is to provide the students with information on molecular spectroscopy and its application for analytical purposes.

Expected learning outcome
After the course, the students are expected to be able to:

• indentify functional groups and identify which form of spectroscopy being able to detection of a given group
• interpret experimental MS, IR and NMR spectra for the indeintification of small, unknown organic molecules by any of the spectroscopical methods or a combination of methods
• combine and value larger amounts of spectroscopic data from the different technices for the purpos of structure determination
• discuss the validity of a suggested molecular structures base don experimental spectra
• solve combined problems on analytical spectroscopy

Subject overview
I. Mass spectrometry (MS):
  1. Introduction to MS

  2. Determination of molecular formula

  3. Fragmentation patterns

  4. Application of MS for identification

II. Infrared spectroscopy (IR):
  1. Introduction to IR spectroscopy

  2. Application of IR spectra for identificatio

III. Magnetic resonance spectroscopy (NMR):
  1. Introduction to NMR spectroscopy

  2. Chemical shift
  3. H-NMR: Spin-spin coupling, Application of 1H-NMR for identification
  4. C-NMR: Application of 13C-NMR for identification

  5. Advanced NMR techniques: DEPT sequence, two-dimensional NMR spectroscopy (COSY spectra, HETCOR technique), application of NMR for identification.


    6. Literature
    • D.L. Pavia, G.M. Lampman og G.S. Kriz: Introduction to Spectroscopy, Harcourt College Publishers, 2001.
    • Analytisk Spektroskopi - Opgaver og øvelsesvejledning , 2004.


    Syllabus
    See syllabus.

    Website
    This course uses e-learn (blackboard).

    Prerequisites for participating in the exam
    None

    Assessment and marking:
    (1) A 4 hour written exam graded according to the Danish 7-point scale and with external evaluation.
    This part is worth 4 ECTS points.

    (2) Obligatory assignements and reports, passed/not passed, internal evaluation by lecturer.
    This part is worth 1 ECTS point.

    Expected working hours
    The teaching method is based on three phase model.

    15 forelæsninger og 11 regneøvelser, obligatorisk laboratorieøvelser (10*2½=25 timer).
    Educational activities

    Language
    This course is taught in Danish.

    Course enrollment
    See deadline of enrolment.

    Tuition fees for single courses
    See fees for single courses.