KE504: Analytical Spectroscopy (5 ECTS)

STADS: 10009701

Level
Bachelor course

Teaching period
The course is held twice a year, once in the autumn semester and once in the spring semester.

Teacher responsible

Email: pcs@sdu.dk

Timetable

Group	Type	Day	Time	Classroom	Weeks
Common	I	Monday	14-15	U55	37,51
Common	I	Tuesday	13-14	U48A	36
Common	I	Tuesday	10-11	U20	38,40,43
Common	I	Wednesday	10-11	U55	38,40,43
Common	I	Wednesday	14-15	U55	41
Common	I	Thursday	10-11	U55	36
Common	I	Thursday	13-14	U55	37-41,43
Common	I	Friday	16-17	U140	36
Common	I	Friday	14-15	U55	39
H2	TL	Wednesday	14-15	Spek	36-37
H2	TL	Wednesday	14-17	Spek	39,44,46,49
H2	TL	Wednesday	14-18	Spek	40,43,45,47
H2	TL	Wednesday	15-18	Spek	41
H2	TL	Wednesday	14-16	Spek	48
H3	TL	Thursday	14-15	Spek	36-37
H3	TL	Thursday	14-17	Spek	39,41,44,46,49
H3	TL	Thursday	14-18	Spek	40,43,45,47
H3	TL	Thursday	14-16	Spek	48
H4	TL	Monday	08-09	Spek	37
H4	TL	Monday	08-11	Spek	39,41,44,46,49
H4	TL	Monday	08-12	Spek	40,43,45,47
H4	TL	Monday	08-10	Spek	48
H4	TL	Thursday	11-12	Spek	36

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Comment:
Kurset afholdes to gange om året, én gang i efteråret og én gang i foråret.

Prerequisites:
None

Academic preconditions:
None

Course introduction
The aim of the course is to provide the students with information on molecular spectroscopy and its application for analytical purposes.

Expected learning outcome
After the course, the students are expected to be able to:

identify functional groups and identify which form of spectroscopy being able to detection of a given group
interpret experimental MS, IR and NMR spectra for the identification of small, unknown organic molecules by any of the spectroscopic methods or a combination of methods
combine and value larger amounts of spectroscopic data from the different techniques for the purpose of structure determination
discuss the validity of a suggested molecular structure based on experimental spectra
solve combined problems on analytical spectroscopy

Subject overview
I. Infrared spectroscopy (IR):

Introduction to IR spectroscopy
Application of IR spectra for identification

II. Mass spectrometry (MS):

Introduction to MS
Determination of molecular formula
Fragmentation patterns
Application of MS for identification

III. Magnetic resonance spectroscopy (NMR):

Introduction to NMR spectroscopy
Chemical shift
H-NMR: Spin-spin coupling, Application of 1H-NMR for identification
C-NMR: Application of 13C-NMR for identification
Advanced NMR techniques: DEPT sequence, two-dimensional NMR spectroscopy (COSY spectra, HETCOR technique), application of NMR for identification.

Literature

D.L. Pavia, G.M. Lampman og G.S. Kriz og J.R. Vyvyan: Introduction to Spectroscopy, 5th ed..
Analytisk Spektroskopi, Opgaver og øvelsesvejledning, seneste udgave..
Software: Tekstbehandling og regneark fra office-pakken el.lign.
Chembiodraw.

Website
This course uses e-learn (blackboard).

Prerequisites for participating in the exam

Participation in lab exercises is a prerequisite for exam part a.
2 E-tests must be passed as a prerequisite for exam part b.

Assessment and marking:

Mandatory assignments and reports, passed/not passed, internal evaluation by teacher (1 ECTS).
Written exam, evaluated by the Danish 7-mark scale by external censorship (4 ECTS).

Reexam in part a: 5 assignments and 5 reports in week 5 for winter-exam and in August for summer-exam.

The mode of exam at the re-examination may differ from the mode of exam at the ordinary exam.

Expected working hours
The teaching method is based on three phase model.
Intro phase: 16 hours
Skills training phase: 36 hours, hereof:
- Tutorials: 11 hours
- Laboratory exercises: 25 hours

Educational activities Study phase: 58 hours

Language
This course is taught in Danish.

Remarks
Tests take 6 h pr. class during the semester

Course enrollment
See deadline of enrolment.

Tuition fees for single courses
See fees for single courses.