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Dansk English

KE504: Analytical Spectroscopy (5 ECTS)

STADS: 10001901

Level
Bachelor course

Teaching period
The course begins in the autumn semester and continues in the spring semester.
1st and 3rd quarter.

Teacher responsible
Email: pcs@dou.dk

Timetable
Group Type Day Time Classroom Weeks Comment
Common I Monday 10-11 U1 05
Common I Monday 10-11 U55 06-09
Common I Tuesday 10-11 U45 05-07
Common I Wednesday 10-11 U1 05
Common I Wednesday 10-11 U45 06-08
Common I Friday 10-11 U55 05-08
S1 TE Monday 09-10 Spektroskopilokalet 06-11
S1 TL Tuesday 08-10 Spektroskopilokalet 06-10
S1 TE Wednesday 11-12 U1 05
S1 TE Wednesday 11-12 U49B 06-09
S1 TL Thursday 14-17 Spektroskopilokalet 06-10
S12 TL Monday 14-16 Spektroskopilokalet 06-10
S12 TE Monday 11-12 U29 06-11
S12 TE Thursday 13-14 Spektroskopilokalet 05-09
S12 TL Thursday 10-13 Spektroskopilokalet 06-10
S14 TE Tuesday 11-12 Spektroskopilokalet 06-11
S14 TL Tuesday 14-16 Spektroskopilokalet 06-10
S14 TE Friday 11-12 Spektroskopilokalet 05-09
S14 TL Friday 12-15 Spektroskopilokalet 06, 08-10
S14 TL Friday 14-17 Spektroskopilokalet 07
T1 TL Monday 12-14 Spektroskopilokalet 06-10
T1 TE Monday 11-12 Spektroskopilokalet 06-11
T1 TE Wednesday 11-12 Spektroskopilokalet 06-10
T1 TL Wednesday 12-15 Spektroskopilokalet 06-10
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Prerequisites:
None

Academic preconditions:
None.

Course introduction
The aim of the course is to provide the students with information on molecular spectroscopy and its application for analytical purposes.

Qualifications
  • to recognize functional groups and to know which spectroscopy form is most suitable for detection of a given group

  • to identify small unknown organic molecules using each single spectroscopic method or a combination of methods

  • to communicate spectroscopic data, orally and in writing

  • to handle and assess large quantities of spectroscopic data
    • Expected learning outcome


    Subject overview
    I. Mass spectrometry (MS):
    1. Introduction to MS

    2. Determination of molecular formula

    3. Fragmentation patterns

    4. Application of MS for identification

    II. Infrared spectroscopy (IR):
    1. Introduction to IR spectroscopy

    2. Application of IR spectra for identificatio

    III. Magnetic resonance spectroscopy (NMR):
    1. Introduction to NMR spectroscopy

    2. Chemical shift
    3. H-NMR: Spin-spin coupling, Application of 1H-NMR for identification
    4. C-NMR: Application of 13C-NMR for identification

    5. Advanced NMR techniques: DEPT sequence, two-dimensional NMR spectroscopy (COSY spectra, HETCOR technique), application of NMR for identification.


      6. Literature
      • D.L. Pavia, G.M. Lampman og G.S. Kriz: Introduction to Spectroscopy, Harcourt College Publishers, 2001.
      • Analytisk Spektroskopi - Opgaver og øvelsesvejledning, 2004.


      Syllabus
      See syllabus.

      Website
      This course uses e-learn (blackboard).

      Prerequisites for participating in the exam
      None

      Assessment and marking:
      Approval of mandatory problems and reports, passed/not passed, internal evaluation by a teacher.
      A 4-hour written examination, external examiner, marks according to the Danish 7-point marking scale.
    Expected working hours
    The teaching method is based on three phase model.

    15 forelæsninger og 11 regneøvelser, obligatorisk laboratorieøvelser (10*2½=25 timer).
    Educational activities

    Language
    This course is taught in Danish.

    Course enrollment
    See deadline of enrolment.

    Tuition fees for single courses
    See fees for single courses.