KE504: Analytical Spectroscopy (5 ECTS)

STADS: 10002101

Level
Bachelor course

Teaching period
The course begins in the autumn semester and continues in the spring semester.
1st and 3rd quarter.

Teacher responsible
Email: pcs@dou.dk

Timetable
Show entire timetable
Show personal time table for this course.

Comment:
OBS! I Eksaminatorietimerne samt lab.timerne vil de studerende blive fordelt på 2 hold. S12 og S13.

Prerequisites:
None

Academic preconditions:
None.

Course introduction
The aim of the course is to provide the students with information on molecular spectroscopy and its application for analytical purposes.

Expected learning outcome
After the course, the students are expected to be able to:

• indentify functional groups and identify which form of spectroscopy being able to detection of a given group
• interpret experimental MS, IR and NMR spectra for the indeintification of small, unknown organic molecules by any of the spectroscopical methods or a combination of methods
• combine and value larger amounts of spectroscopic data from the different technices for the purpos of structure determination
• discuss the validity of a suggested molecular structures base don experimental spectra
• solve combined problems on analytical spectroscopy

Subject overview
I. Mass spectrometry (MS):

1. Introduction to MS


2. Determination of molecular formula


3. Fragmentation patterns


4. Application of MS for identification

II. Infrared spectroscopy (IR):

1. Introduction to IR spectroscopy


2. Application of IR spectra for identificatio

III. Magnetic resonance spectroscopy (NMR):

1. Introduction to NMR spectroscopy


2. Chemical shift
3. H-NMR: Spin-spin coupling, Application of 1H-NMR for identification
4. C-NMR: Application of 13C-NMR for identification


5. Advanced NMR techniques: DEPT sequence, two-dimensional NMR spectroscopy (COSY spectra, HETCOR technique), application of NMR for identification.


Literature

• D.L. Pavia, G.M. Lampman og G.S. Kriz: Introduction to Spectroscopy, Harcourt College Publishers, 2001.
• Analytisk Spektroskopi - Opgaver og øvelsesvejledning, 2004. .


Syllabus
See syllabus.

Website
This course uses e-learn (blackboard).

Prerequisites for participating in the exam
None

Assessment and marking:
(1) A 4 hour written exam graded according to the Danish 7-point scale and with external evaluation.
This part is worth 4 ECTS points.

(2) Obligatory assignements and reports, passed/not passed, internal evaluation by lecturer.
This part is worth 1 ECTS point.

Expected working hours
The teaching method is based on three phase model.

15 forelæsninger og 11 regneøvelser, obligatorisk laboratorieøvelser (10*2½=25 timer).
Educational activities

Language
This course is taught in Danish.

Course enrollment
See deadline of enrolment.

Tuition fees for single courses
See fees for single courses.