KE504: Analytical Spectroscopy (5 ECTS)

STADS: 10008001

Level
Bachelor course

Teaching period
The course is held twice a year, once in the autumn semester and once in the spring semester.

Teacher responsible
Email: pwj@sdu.dk

Timetable
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Prerequisites:
None

Academic preconditions:
Students from the Faculty of Science: KE501/K-501/KC-501 or FF504 or FF503 must be passed
Students from the Faculty of Engineering: Fundamental Chemistry must be passed.

Course introduction
The aim of the course is to provide the students with information on molecular spectroscopy and its application for analytical purposes.

Expected learning outcome
After the course, the students are expected to be able to:

• identify functional groups and identify which form of spectroscopy being able to detection of a given group
• interpret experimental MS, IR and NMR spectra for the identification of small, unknown organic molecules by any of the spectroscopic methods or a combination of methods
• combine and value larger amounts of spectroscopic data from the different techniques for the purpose of structure determination
• discuss the validity of a suggested molecular structure based on experimental spectra
• solve combined problems on analytical spectroscopy

Subject overview
I. Infrared spectroscopy (IR):

1. Introduction to IR spectroscopy
2. Application of IR spectra for identification

II. Mass spectrometry (MS):

1. Introduction to MS
2. Determination of molecular formula
3. Fragmentation patterns
4. Application of MS for identification

III. Magnetic resonance spectroscopy (NMR):

1. Introduction to NMR spectroscopy
2. Chemical shift
3. H-NMR: Spin-spin coupling, Application of 1H-NMR for identification
4. C-NMR: Application of 13C-NMR for identification
5. Advanced NMR techniques: DEPT sequence, two-dimensional NMR spectroscopy (COSY spectra, HETCOR technique), application of NMR for identification.

Literature

• D.L. Pavia, G.M. Lampman og G.S. Kriz og J.R. Vyvyan: Introduction to Spectroscopy, 4th ed., Harcourt College Publishers, 2009.
• Analytisk Spektroskopi: Opgaver og øvelsesvejledning, seneste udgave.Ligger på E-learn
• Software: Tekstbehandling og regneark fra office-pakken el.lign.
• Chembiodraw .

Website
This course uses e-learn (blackboard).

Prerequisites for participating in the exam
None

Assessment and marking:

1. Obligatory assignments and reports, passed/not passed, internal evaluation (1 ECTS)
2. Multiple choice-tests and reports, passed/not passed, internal evaluation (4 ECTS). This consist of the following:
1. digital test 1,
2. digital test 2,
3. Identification rapport

Reexam in the same exam period or immediately thereafter. The mode of exam at the re-examination may differ from the mode of exam at the ordinary exam.

Expected working hours
The teaching method is based on three phase model.
Intro phase: 16 hours
Skills training phase: 34 hours, hereof:
 - Tutorials: 10 hours
 - Laboratory exercises: 24 hours

Educational activities Study phase: 58 hours

Language
This course is taught in Danish.

Remarks
Tests takes 6 h pr. class during the semester 

Course enrollment
See deadline of enrolment.

Tuition fees for single courses
See fees for single courses.