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Dansk English

KE504: Analytical Spectroscopy (5 ECTS)

STADS: 10009701

Level
Bachelor course

Teaching period
The course is held twice a year, once in the autumn semester and once in the spring semester.

Teacher responsible
Email: pcs@sdu.dk

Timetable
Group Type Day Time Classroom Weeks Comment
Common I Monday 10-11 U155 5
Common I Tuesday 10-11 U155 5
Common I Tuesday 14-15 U155 6-7,13,20
Common I Tuesday 16-17 U155 10
Common I Wednesday 10-11 U155 5,9-10,13
Common I Wednesday 09-10 U155 6-7
Common I Wednesday 14-15 U156 11
Common I Thursday 16-17 U155 9
Common I Thursday 14-15 U154 11
H1 TL Monday 12-13 Spek 7
H1 TL Monday 16-17 Spek 9
H1 TL Tuesday 12-15 Spek 10,15,17
H1 TL Tuesday 16-18 Spek 19
H1 TL Wednesday 08-12 Spek 14,16,18
H1 TL Wednesday 08-11 Spek 20
H1 TL Thursday 08-12 Spek 11
H1 TL Thursday 09-12 Spek 13
H2 TL Monday 13-14 Spek 7
H2 TL Monday 17-18 Spek 9
H2 TL Monday 13-16 Spek 10,15,17
H2 TL Monday 13-17 Spek 11,14,16,18
H2 TL Tuesday 08-10 Spek 19
H2 TL Wednesday 15-18 Spek 13,20
H3 TL Monday 14-15 Spek 7
H3 TL Monday 15-16 Spek 9
H3 TL Monday 08-12 Spek 16
H3 TL Wednesday 14-17 Spek 10,17
H3 TL Thursday 12-14 Spek 19
H3 TL Thursday 12-15 Spek 20
H3 TL Friday 10-14 Spek 11,14,18
H3 TL Friday 10-13 Spek 13
H3 TL Friday 09-12 Spek 15
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Prerequisites:
None

Academic preconditions:
None

Course introduction
The aim of the course is to provide the students with information on molecular spectroscopy and its application for analytical purposes.

Expected learning outcome
After the course, the students are expected to be able to:

  • identify functional groups and identify which form of spectroscopy being able to detection of a given group
  • interpret experimental MS, IR and NMR spectra for the identification of small, unknown organic molecules by any of the spectroscopic methods or by a combination of methods
  • combine and value larger amounts of spectroscopic data from the different techniques for the purpose of structure determination
  • discuss the validity of a suggested molecular structure based on experimental spectra
  • solve combined problems on analytical spectroscopy
Subject overview
I. Infrared spectroscopy (IR):

  1. Introduction to IR spectroscopy
  2. Application of IR spectra for identification

II. Mass spectrometry (MS):

  1. Introduction to MS
  2. Determination of molecular formula
  3. Fragmentation patterns
  4. Application of MS for identification

III. Magnetic resonance spectroscopy (NMR):

  1. Introduction to NMR spectroscopy
  2. Chemical shift
  3. H-NMR: Spin-spin coupling, Application of 1H-NMR for identification
  4. C-NMR: Application of 13C-NMR for identification
  5. Advanced NMR techniques: DEPT sequence, two-dimensional NMR spectroscopy (COSY spectra, HETCOR technique), application of NMR for identification.
Literature
  • D.L. Pavia, G.M. Lampman og G.S. Kriz og J.R. Vyvyan: Introduction to Spectroscopy, 5th ed.
  • Analytisk Spektroskopi, Opgaver og øvelsesvejledning , seneste udgave.
  • Software: Tekstbehandling og regneark fra office-pakken el.lign. .
  • Chembiodraw.


Website
This course uses e-learn (blackboard).

Prerequisites for participating in the exam
  1. Participation in lab exercises is a prerequisite for exam part a.
  2. 2 E-tests must be passed as a prerequisite for exam part b.

Pass/fail, internal evaluation by teacher.



Assessment and marking:
  1. Mandatory assignments and reports, passed/not passed, internal evaluation by teacher (1 ECTS).
  2. Written exam, evaluated by the Danish 7-mark scale by external censorship (4 ECTS).

Reexam in part a: 5 assignments and 5 reports the week before exam b for winter-exam and in August for summer-exam.

The mode of exam at the re-examination may differ from the mode of exam at the ordinary exam.



Expected working hours
The teaching method is based on three phase model.
Intro phase: 16 hours
Skills training phase: 36 hours, hereof:
 - Tutorials: 11 hours
 - Laboratory exercises: 25 hours

Educational activities

Language
This course is taught in Danish.

Remarks
Tests take 6 hours per class during the semester.

Course enrollment
See deadline of enrolment.

Tuition fees for single courses
See fees for single courses.