KE822: Organic chemical analysis and separation (5 ECTS)

STADS: 10010401

Level
Master's level course

Teaching period
The course is offered in the autumn semester.
The course takes place in the second part of the autumn semester.

Teacher responsible
Email: erik@sdu.dk

Timetable
Show entire timetable
Show personal time table for this course.

Comment:
Samlæses med bachelorkurset KE510. Labhold kommer senere.

Prerequisites:
None

Academic preconditions:
Analytical spectroscopy (KE504) and Organic Chemistry (KE505) are presupposed known

Course introduction
The students should obtain practical skills in separating substance mixtures by using modern separation and purification techniques and obtain practical skills in identifying and determining the functional groups of organic substances. Through identification of IR, MS and 1H and 13C NMR spectra the students should be trained in practical analytical molecular spectroscopy including the interpretation problems implied in the fact that substances could be impure or poorly separated

Expected learning outcome

• Use chemical methods for identification of organic compounds.
• Use spectroscopic methods for identification of organic compounds.
• Use chemical and column chromatographic separation techniques.
• Carry out small scale chemical reactions.
• Find reference data on-line.
• Knowledge of gas chromatography and HPLC.
• Estimate purity of a chemical sample.

Subject overview
Separation of substance mixtures by extraction and preparative column chromatography. Preparation of derivatives. Determination of functional groups and equivalent weight. HPLC and GLC analysis. Identification by MS, 1H and 13C NMR and IR spectra.

Literature

Øvelsesvejledning der placeres på Blackboard

Website
This course uses e-learn (blackboard).

Prerequisites for participating in the exam
Active participation in laboratory exercises and handing in of two reports is a prerequisite for participating in evaluation a.

Assessment and marking:

1. Approval of written report graded according to the 7-scale. External censorship (5 ECTS).

Reexam in January.
The mode of examination at the reexamination may differ from the mode of exam at the ordinary examination.

Expected working hours
The teaching method is based on three phase model.
Intro phase: 1 hours
Skills training phase: 49 hours, hereof:
 - Laboratory exercises: 49 hours

Educational activities

Language
This course is taught in English, if international students participate. Otherwise the course is taught in Danish.

Remarks
Co-taught with the corresponding bachelor course KE510. The course is an introduction to practical organic separation. Therefore it is recommended to attend this course before a project in organic chemistry.

The course runs over a 4 week period in weeks 48-51.

Course enrollment
See deadline of enrolment.

Tuition fees for single courses
See fees for single courses.